Scientific Highlights

Cover Materials Today

Operando X-ray diffraction during laser 3D printing

Ultra-fast operando X-ray diffraction experiments reveal the temporal evolution of low and high temperature phases and the formation of residual stresses during laser 3D printing of a Ti-6Al-4V alloy. The profound influence of the length of the laser-scanning vector  on the evolving microstructure is revealed and elucidated.  

covid-19

SLS MX beamtime update

Update of the SLS MX beamline operation during the COVID-19 period

Innovation Award on Synchrotron Radiation 2019 for the development of XFEL detectors using the adaptive gain principle

Innovation Award on Synchrotron Radiation 2019 for the development of XFEL detectors using the adaptive gain principle

The Innovation Award on Synchrotron Radiation 2019 was given to the researchers Prof. Heinz Graafsma from Desy and Dr. Aldo Mozzanica and Dr. Bernd Schmitt both from the Paul Scherrer Institute. The three physicists were honored for their contributions to the development of detectors for XFEL applications based on the dynamic gain switching principle enabling simultaneously single photon resolution and a large dynamic range. The laudation was held by Prof. Edgar Weckert from Desy. The Synchrotron Radiation Innovation Award is sponsored by SPECS GmbH and BESTEC GmbH.

Illustration of the crystal structure of (MA)PbBr3

Ultrafast diffuse x-ray scattering of a hybrid perovskite crystal

Organic–inorganic ‘hybrid’ perovskites have recently gained attention as a low-cost alternative to silicon solar cells. However, many properties of these materials are still poorly understood. In particular, how imperfections in the crystals, which can be both static or dynamic, affect energy transport remains unclear.

ExPaNDS partners meet at the grant kick-off meeting in September 2019

New 6M€ European grant awarded to ExPaNDS to drive open access data

A new 6M€ grant is being launched for the Photon and Neutron Data Services (ExPaNDS) to come together and work under the European Open Science Cloud (EOSC). This ambitious project will create enormous opportunities for scientific communities, and through their findings for humankind worldwide. It aims to publish and map the data behind the thousands of successful published scientific papers generated by Europe’s Photon and Neutron Research Infrastructures (PaN RIs) – which every year create petabytes of data – and make it available to all.

PSI School for Masterstudents 2019

PSI School for Master Degree Students - Introducing Photons, Neutrons and Muons for Condensed Matter Physics and Materials Science

From 17 – 21 June 2019 the Neutron and Muon Division (NUM) and the Photon Science Division (PSD) of PSI hosted 18 Master Degree students of physics, chemistry, materials and interdisciplinary science, as well as nuclear engineering to provide an introduction to the characterization of materials with large scale facilities like SINQ, SμS, SLS and SwissFEL. The course taught a basic understanding of how photons, neutrons and muons interact with matter, and how this knowledge can be used to solve specific problems in materials research.

Details of the program can be found at http://indico.psi.ch/event/PSImasterschool

Measured longitudinal phase space of the injected electron beam

First serial femtosecond crystallography experiment using SwissFEL’s large bandwidth X-ray pulses

The typical mode of operation at XFEL facilities uses the so-called self-amplified spontaneous emission (SASE) process to generate the short, bright X-ray pulses. This mode of operation is stochastic in nature, causing some variance in intensity and spectrum on a shot-to-shot basis, which makes certain types of crystallographic measurements much more challenging.

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HERCULES school 2019 at SLS

In the week of April 1-5 PSI welcomes 20 PhD students and postdocs taking part in the European HERCULES 2019 school on Neutron and Synchrotron Radiation. They will attend lectures and perform two days of practical courses at several beam lines of the Swiss Light Source.

Figure 1. Layout depicting the experimental conditions at the Alvra experimental station. (b) Fresnel simulation of the Talbot carpet: intensity distribution of the experimental conditions for a 1D diamond phase grating with a 200 nm pitch and 2.985 keV photon energy. The inset (c) shows the detailed structure of the interference pattern in the vicinity of the sample where the pitch is 190 nm

Towards X-ray Transient Grating Spectroscopy at SwissFEL

The high brilliance of new X-ray sources such as X-ray Free Electron Laser opens the way to non-linear spectroscopies. These techniques can probe ultrafast matter dynamics that would otherwise be inaccessible. One of these techniques, Transient Grating, involves the creation of a transient excitation grating by crossing X-ray beams on the sample. Scientists at PSI have realized a demonstration of such crossing by using an innovative approach well suited for the hard X-ray regime.

Dr Yasin Ekinci elected as Fellow of SPIE

Dr. Yasin Ekinci, Head of the Advanced Lithography and Metrology Group and ad interim Head of the Laboratory for Micro and Nanotechnology, has been elected to the grade of Fellow of The International Society for Optics and Photonics (SPIE).

SESAME beamline for tomography project (BEATS) is launched

On 1st January 2019, the European Horizon 2020 project BEAmline for Tomography at SESAME (BEATS) was launched with the objective to design, procure, construct and commission a beamline for hard X-ray full-field tomography at the SESAME synchrotron in Jordan. The European grant is worth 6 million euros and will span a four-year period from beginning 2019 to end 2022.

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Dr Mirjam van Daalen appointed as Swiss ESFRI delegate

Dr. Mirjam van Daalen Chief of staff of the Photon Science Division, was mandated on the 1st of January 2019, by the State Secretariat for Education, Research and Innovation SERI as a member of the Swiss Delegation to the European Science Forum on Research Infrastructures ESFRI https://www.esfri.eu/.

First femtosecond protein pump-probe measurements at SwissFEL

A major milestone in the commissioning of SwissFEL has been reached: the first pump-probe experiments on proteins have been successfully carried out. Crystals of several retinal-binding proteins were delivered in a viscous jet system and a femtosecond laser was used to start the isomerization reaction. Microsecond to sub-picosecond snapshots were then collected, catching the retinal proteins shortly after isomerization of the chromophore.

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2018 Innovation Award on Synchrotron Radiation

The Innovation Award on Synchrotron Radiation 2018 went to Dr. Christian David, also from the Paul Scherrer Institute, and to Prof. Alexei Erko, who recently moved from the HZB to the Institute for Applied Photonics (IAP) in Berlin-Adlershof.

3D rendering of hierarchically-structured monolithic nanoporous gold with approx. 23 nm spatial resolution obtained by ptychographic X-ray tomography, showing binary representation of gold and pores after image segmentation (above) and the resulting orthographic projection (below).

Helping chemists to understand degradation and stabilization of catalytic nanoporous gold structures

Catalytic materials are ubiquitously used in industrial processes to perform chemical reactions efficiently and in a sustainable manner. Nanoporous gold (npAu) is a monolithic sponge-like catalyst exhibiting a hierarchical structure with pores and connecting ligaments of typically 10 to 50 nm.

SwissFEL's First Call for Proposals

The first SwissFEL call for proposals took place, deadline for submission was the 15th of September. In this first call for proposals SwissFEL received overwhelming interest from the user community. A total of 47 proposals were submitted for the SwissFEL Alvra experimental station and 26 for the Bernina experimental station. The Proposal Review committee PRC took place on 18-19 October 2018.

(a) Scanning transmission x-ray microscopy images of magnetic skyrmions stabilized in a nanostructured Pt/Co/Ir disc; (b) Skyrmion-dependent contribution to the Hall resistivity

Discrete Hall contribution of magnetic skyrmions

The reliable electrical detection of magnetic skyrmions is of fundamental importance for the application of such topological magnetic quasi-particles for data storage devices. Researchers in a joint collaboration between the University of Leeds and the PolLux endstation have investigated the electrical detection of isolated magnetic skyrmions in applications-relevant nanostructured devices, observing the presence of a strong skyrmion-dependent contribution to the Hall resistivity.

Demonstration of femtosecond X-ray pump X-ray probe diffraction on protein crystals

Our experiments, published in the September issue of Structural Dynamics, demonstrate the feasibility of time-resolved pump-multiprobe X-ray diffraction experiments on protein crystals using a split-and-delay setup which was temporarily installed at the LCLS X-ray Free Electron Laser.

Diamond: a gem for micro-optics

Our image of a diamond structure was published on the cover page of the September 2018 issue of the journal "Materials Today". The corresponding paper reports on the nano-frabrication of micro-optical elements in diamond.

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Claire Donnelly dissertation research awards

Claire Donnelly, Mesoscopic Systems (ETH Zurich - PSI), was awarded the COMSOL SPS Award in Computational Physics, the Werner Meyer-Ilse Memorial Award, the ETH Medal for an outstanding doctoral thesis, and the American Physical Society Richard L. Greene Dissertation Award.

MOOCs – a paradigm shift in education

In March 2018, the nine-week MOOC “Introduction to synchrotrons and x-ray free-electron lasers” (abbreviated to “SYNCHROTRONx”) came online via the edX provider of the École Polytechnique Fédérale de Lausanne (EPFL), created by Phil Willmott of the Swiss Light Source, Paul Scherrer Institute. “MOOC” is an acronym for “massive open online course”, a teaching platform started in the first decade of this century, which has become increasingly popular in the last five to six years. MOOCs have no limits to participation and are free. Some of the most popular MOOCs can attract many tens of thousands of participants. Even the most specialized subjects may have an initial enrollment of over a thousand, more than an order of magnitude larger than that typically found in traditional higher education. There were over 70 million MOOC enrollments covering nearly 10’000 subjects offered by the top five providers in 2017 alone!

Creation and deletion of isolated magnetic skyrmions via electrical currents

The writing and deletion of magnetic Skyrmions is a fundamental step towards the fabrication of memory devices based on this promising spin configuration. Researchers at the Korea Institute of Technology have demonstrated the writing and deleting of isolated magnetic Skyrmions at room temperature in ferrimagnetic multilayer superlattice stacks using electrical currents.

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Fresnel Zone Plates with Zone Widths below 10 nm

The spot size of a Fresnel Zone Plate lens is mainly determined by the zone widths of its outermost zone. It is therefore essential to fabricate zone plates with structures as small as possible for high-resolution X-ray microscopy. Researchers at the Laboratory for Micro- and Nanotechnology at the PSI have now developed Fresnel zone plates with zone widths well below 10 nm, down to 6.4 nm. These lenses are capable of pushing resolution in X-ray microscopy to the single-digit regime.

Dr. Caterina Biscari, Director of the ALBA Synchrotron in Spain and Vice Chair of LEAPS, League of European Accelerator-based Photon Sources, presented the LEAPS Strategy 2030 to Jean-David Malo, Director, Directorate General Research and Innovation, European Commission

LEAPS join forces with the European Commission to strengthen Europe’s leading role in science

“A world where European science is a catalyst for solving global challenges, a key driver for competitiveness and a compelling force for closer integration and peace through scientific collaboration.” This is the vision of LEAPS, League of European Accelerator-based Photon Sources, on which the LEAPS Strategy 2030 is based. Director Jean-David Malo, DG Research and Innovation, received the strategy today at the Bulgarian Presidency Flagship Conference on Research Infrastructures.

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HERCULES at the Swiss Light Source

In the week of March 18-23 PSI welcomes 20 PhD students and postdocs taking part in the HERCULES 2018 school on Neutron and Synchrotron Radiation. They will attend lectures and perform two days of practical courses at several beam lines of the Swiss Light Source.

Left: X-ray absorption spectra from supersaturated calcium carbonate solutions taken with a liquid microjet at the PHOENIX beamline. Comparison of the spectra with theoretical modeling shows the dominance of various ion pairs in solution, as expected in a classical solution. Right: image of liquid microjet in PHOENIX endstation.

Are supersaturated calcium carbonate solutions classical or non-classical ?

Classical theory predicts that supersaturated carbonate solutions consist mostly of ions and ion pairs, with a small number of larger clusters present in the solution. The population of the different sized clusters in a solution is solely defined by the cluster’s size dependent Free Energy. If clusters are large enough they serve as nucleation germs for a new solid phase. The nucleation occurs once the surface free energy barrier posed by the new solid-liquid interface is overcome by the free energy win from bulk phase growth.

Modulation data

Unravelling structure sensitivity in CO2 hydrogenation over nickel

Using a unique set of well-defined silica-supported Ni nanoclusters (1–7 nm) and advanced characterization methods it was proved how structure sensitivity influences the mechanism of catalytic CO2 reduction, the nature of which has been long debated.

First Pilot Experiment at SwissFEL-Alvra: UV photo-induced charge transfer in OLED system

On the 17th of December 2017 SwissFEL saw its first pilot experiment in the Alvra experimental station of the SwissFEL ARAMIS beamline.

First time resolved Pilot Experiment by SwissFEL: Semiconductor to metal transition in Ti3O5 nanocrystals

On the 30th of November 2017 SwissFEL saw its first time resolved pilot experiment in the Bernina experimental station of the SwissFEL ARAMIS beamline. A team of scientists from the University of Rennes, ESRF and PSI, led by Marco Cammarata (Univ. Rennes) and Henrik Lemke (PSI), successfully started the experimental phase at SwissFEL.