Lab News & Scientific Highlights

In situ alloying is an effective method to engineer microstructures of additively manufactured Ti6Al4V3Fe alloys. 

We present a novel monitoring strategy for 3D print processes that consists of developing and training a hybrid machine learning model that can classify regimes across different time scales based on heterogeneous sensing data. 

The mechanochromism of hybrid 2D perovskites is probed at pressures compatible with practical applications

Polyoxomolybdates have been directly synthesized from basic reagents in a mechanochemical one-pot reaction.

Aerosols in the atmosphere react to incident sunlight. This light is amplified in the interior of the aerosol droplets and particles, accelerating reactions. ETH and PSI researchers have now been able to demonstrate and quantify this effect and recommend factoring it into future climate models.

The reaction of elemental scandium and zirconium powders with liquid aluminum is observed directly via operando X-ray diffraction during laser 3D printing. This work demonstrates that elemental blends can be used to create fine-grained crack-free Al-alloys and highlights the importance of feature size.

Combining time-resolved soft X-ray STXM imaging with magnetic laminography, researchers were able to investigate magnetization dynamics in a ferromagnetic microstructure resolved in all three spatial dimensions and in time. Thanks to the possibility of freely selecting the frequency of the excitation applied to the magnetic element, this technique opens the possibility to investigate resonant magneto-dynamical processes, such as e.g. magnetic vortex core gyration and switching, and spinwave emission.

PSI hosted again the Hercules School in March 2022. We had the pleasure to welcome 20 international PhD students, PostDocs and scientists to demonstrate our state-of-the-art techniques and methodologies at our large scale facilities, the Swiss Light Source (SLS), the Swiss Spallation Neutron Source (SINQ) and our free electron laser SwissFEL.

A novel approach to controlling the speed of magnetic processes has been found through resonant magnetic scattering in an antiferromagnetic Lanthanide intermetallics.

Operando high-speed X-ray radiography experiments reveal the cracking mechanism during 3D laser printing of a Ni superalloy.

Synchrotron X-ray diffraction experiments reveal the presence of a non- negligible amount of tetragonal phase in 3D printed red-gold samples. 

Scientists have used state-of-the-art 3D printing and microscopy to provide a new glimpse of what happens when taking magnets to three-dimensions on the nanoscale – 1000 times smaller than a human hair.

In an interdisciplinary project, researchers from the Laboratory of Nanoscale Biology in BIO  and the Laboratory for Condensed Matter in PSD have revealed the reaction between the nitrogen atoms of the amyloid-beta peptide and copper/zinc ions by using soft X-ray absorption spectroscopy.

This experiment performed at SwissFEL shows how fast we can localize electrons out of an electron gas into correlated, well localized states of a material. It is based on a combined ultrafast x-ray absorption and diffraction experiment on an intermetallic system.

Within this synergetic collaboration, PSI scientists have investigated the correlation between magnetic and electronic ordering in NdNiO3 by tuning its properties through proximity to a ferromagnetic manganite layer. The main outcome is that the stray magnetic field from the manganite layer causes a novel ferromagnetic-metallic (FM-M) phase in NNO. This work demonstrates the utilization of heterostructure engineering for creating novel quantum phases.

The authors demonstrate the stability of ferromagnetic order of one unit cell thick optimally doped manganite (La0.7Ba0.3MnO3, LBMO) epitaxially grown between two layers of SrRuO3 (SRO). LBMO shows ferromagnetism even above SRO Tc. Density Functional Theory calculations help understand the reasons behind this interesting result.

During the week of March 15 – 19, we had the pleasure to welcome 20 international PhD students, PostDocs and assistant professors at PSI, taking part in the first virtual HERCULES SCHOOL on Neutrons & Synchrotron Radiation.

Employing time-resolved STXM imaging, researchers investigated the emission of spin waves from a magnetic vortex core. By applying static magnetic fields, the control of both the shape of the vortex core and of the spatial profile of the emitted spin waves could be demonstrated, allowing for the fabrication of field-tunable spin wave focusing elements.

The authors find that an annealing process can create a highly ordered network of two-dimensional line defects at the buried interface between a relaxed film and its substrate. The low dimensional network spacing is directly related to the lattice mismatch and can correspondingly be tuned by the choice of substrate.