Beamline Optics

A document describing the optics geometry for the new setup for undulator radiation is described here 

 

The optical elements of the beamline and their functions are listed here.

ElementFunctionDistance from source [m]
FilterBeam attenuation18.8
Optics slitsBeam definition19.2
XBPM1Beam position monitoring19.4
First LN2 cooled DCM crystalMonochromatization20.142
Second DCM crystalHorizontal focussing20.2-20.5
XBPM2Beam position monitoring20.69
Mirror 1Vertical collimation21.514
Mirror 2Vertical focussing22.214
XBPM3Beam position monitoring23.3
Station shutterExtinction of experimental beam23.772
Bremsstrahlung blockerBlocking of direct beam and BS30.485
EH1 slitsBeam definition30.9

The double crystal monochromator (DCM) consists of two Si 111 crystals which are precisely positioned and oriented in the X-ray beam.

View inside the DCM
View inside the DCM
DCM motor movements

Two successive Bragg reflections, with an inherent energy resolution of 0.014 %, direct photons of the desired energy parallel to the incoming beam direction, but offset downward (out of the direct Bremsstrahlung beam) by 15 mm. Changes in photon energy require changes in the mirror angle and hence in the height of the DCM. 

The polychromatic incoming beam (shown here as white) is monochromated by the first Si-crystal. The second Si-crystal is nominally set at the same angle and can be moved along a translation stage such that the outgoing beam (here, blue) is 15 mm lower in height than the incoming beam. 

_An aperture 90 cm downstream allows the monochromated beam to pass, but blocks any high-energy Bremsstrahlung transmitted at the original height of 1400 mm. The large heat load absorbed by the first DCM crystal (up to 1 kW) causes it to deform, and a mechanical bending apparatus, ("TORII", developed at Hasylab), dynamically corrects this curvature._ The second crystal provides sagittal focusing; it is a ribbed crystal, cylindrically bent to a variable curvature radius (Rmin=1 m) in a flexure-hinge fixture developed at the ESRF. 

The DCM motors are controlled by EPICS channel widgets. A schematic of the motor movements and a table listing their functions are shown here. 

The outgoing beam is shifted up by 20 mm compared to the incoming beam. See Table below for the motor functions.

EPICS channelDescription
First crystal 
MOX1:ROXrotation (pitch) of the first crystal stages around X axis
MOX1:ROYrotation (roll) of the first crystal stages around Y axis
MOX1:TRYtranslation of 1st crystal stage
Second crystal 
MOX2:ROXfine adjustment of Bragg angle of 2nd crystal
MOX2:ROYroll of 2nd crystal
MOX2:ROZyaw of 2nd crystal
MOX2:TRXyaw of second crystal around its normal
MOX2:TRYvertical movement
MOX2:TRZhorizontal translation of 2nd crystal
MOX2:TRYA...Dflexing of 2nd crystal to produce sagittal (horizontal) focussing
1st and 2nd Mirror

The beamline optics are shown below. The first mirror (MI1) provides vertical collimation and removes high-order harmonics. The mirror consists of a 1 m long Si blank, Rh-coated (K-edge: 23 keV), which can be tilted up to 5 mrad and bent (5 < R < 30 km) as required for the desired photon energy. The surface of the mirror has been polished to a rms roughness less than 0.5 nm and to a rms residual slope error less than 2.5 m rad. 

The second mirror (MI2) is similar to MI1. A variable curvature permits vertical focusing at the experimental station in use. Since this focusing introduces a vertical divergence, which is undesirable, for example, in high-resolution powder diffraction, the user may choose to either set the radius of curvature to infinity or to remove MI2 from the beam altogether, the latter option causing an inclined beam. 
 

Below are graphs and formulae for the optimal seetings for horizontal (sagittal) focussing of the second DCM crystal for different energies at the powder and surface diffraction stations.